The influence of annealing on the crystallization and tribological behavior of MWNT/PEEK nanocomposites

In this study, annealing influence on crystallization and scratch behavior of neat and multi‐wall carbon nanotube (MWNT) reinforced poly(ether ether ketone) (PEEK) nanocomposites have been investigated. Crystallization behavior of normal and annealed samples was investigated by using differential scanning calorimeter (DSC). Scratch behavior of normal and annealed samples was investigated by using micro scratch tester. In DSC analysis, it was detected that, melting enthalpy of annealed neat PEEK was increased sharply when compared to neat PEEK. Melting enthalpies of annealed PEEK nanocomposites prepared with addition of up to 1 wt% MWNT were increased with a decreased trend. However, nanocomposites with higher contents of MWNTs (>1 wt%) were dramatically affected by annealing process and melting enthalpy decreased sharply. Friction coefficient values of “annealed MWNT reinforced PEEK composites” were found to be lower than “normal PEEK composites.” Annealing process affects scratch hardness of both annealed and MWNT reinforced PEEK. Annealed nanocomposites with various MWNT concentrations showed higher scratch hardness values than normal PEEK nanocomposites. POLYM. COMPOS., 2011. © 2011 Society of Plastics Engineers     

Wake-up receivers for wireless sensor networks: benefits and challenges - [Accepted from open call]

For successful data delivery, the destination nodes should be listening to the medium to receive data when the sender node starts data communication. To achieve this synchronization, there are different rendezvous schemes, among which the most energy-efficient is utilizing wakeup receivers. Current hardware technologies of wake-up receivers enable us to evaluate them as a promising solution for wireless sensor networks. In this article the benefits achieved with wake-up receivers are investigated along with the challenges observed. In addition, an overview of state-of-the-art hardware and networking protocol proposals is presented. As wake-up receivers offer new opportunities, new potential application areas are also presented and discussed.     

Activation of glassy carbon electrodes by photocatalytic pretreatment

This paper describes a simple and rapid photocatalytic pretreatment procedure that removes contaminants from glassy carbon (GC) surfaces. The effectiveness of TiO₂ mediated photocatalytic pretreatment procedure was compared to commonly used alumina polishing procedure. Cyclic voltammetric and chronocoulometric measurements were carried out to assess the changes in electrode reactivity by using four redox systems. Electrochemical measurements obtained on photocatalytically treated GC electrodes showed a more active surface relative to polished GC. In cyclic voltammograms of epinephrine, Fe(CN)₆^3−/4− and ferrocene redox systems, higher oxidation and reduction currents were observed. The heterogeneous electron transfer rate constants (k^o) were calculated for Fe(CN)₆^3−/4− and ferrocene which were greater for photocatalytic pretreatment. Chronocoulometry was performed in order to find the amount of adsorbed methylene blue onto the electrode and was calculated as 0.34 pmol cm⁻² for photocatalytically pretreated GC. The proposed photocatalytic GC electrode cleansing and activating pretreatment procedure was more effective than classical alumina polishing.     

Post-buckling behavior of carbon fiber epoxy composite plates

In this study, the pre-buckling and post-buckling behaviors of layered composite plates which were made of woven carbon fiber fabric with a circular hole in the middle were investigated experimentally and numerically. Firstly, load-displacement graphs of composite plates with different hole diameters were experimentally obtained under compressive load. Then the numerical load-displacement graphs of the plates were found with the ANSYS package program which used the finite element method. As a result, after linear buckling experimental and numerical results were found to be compatible with each other. In addition, damage behavior of plates after buckling with the aid of Tsai-Wu damage criterion was obtained similar to experimental results. The increase in hole diameter did not change the load-displacement behavior characteristics of the plates after buckling. However, it has reduced maximum damage load and maximum failure displacement. The stress at the perimeter of the hole increased significantly with the increase of the vertical displacement with immediately after the buckling but later was not significantly affected by this increase.

     

Diversity and functional characteristics of lactic acid bacteria from traditional kefir grains

Traditional kefir grains were collected from distinct parts of Turkey, and their microbial profile was determined. A wide bacterial biota was observed formed by distinct lactic acid bacteria (LAB) in which Lactococcus lactis strains appeared to be dominant. Yeast species were also identified in kefir grains. Significant levels of antifungal and antibacterial activities were monitored in kefir isolates. All tested LAB produced an exopolysaccharide (EPS) containing glucose and galactose, and some strains formed a fructan‐type EPS. Importantly, low levels of antibiotic resistance were observed among the kefir isolates.     

Novel ZA27/B4C/Graphite Hybrid Nanocomposite-Bearing Materials with Enhanced Wear and Corrosion Resistance

Metallurgical and Materials Transactions A - In this study, nanosized B4C and graphite-reinforced ZA27 matrix hybrid nanocomposites were produced with mechanical milling followed by hot pressing....     

Theoretical and experimental investigation of effects of failures on the tensile endurance of elevator ropes

Elevators have an important place in human life just after uprising demands in high rise buildings, skyscraper and luxury residence concepts have surged. Steel wire ropes provide permanent working safety and reliability in the elevator installations. Due to this reason steel wire ropes are one of the vital components of elevators. In this study, effects of discard criteria such as wire breaks, abrasive wear and corrosion where extents of those failures are defined by ISO 4344 standard on the tensile endurance of 6×19 Seale and 8×19 Warrington elevator ropes have been investigated theoretically and experimentally. Tensile endurances of rope samples that have different extents of failure have been determined by using tensile testing machine and comparison is made by undamaged samples for each rope separately. In addition, stress and strain values occurred on the elevator ropes investigated have also been presented. The most critical failure type has been found to be 24 wire breaks for 6×19 Seale rope with fiber core where lifting capacity reduced by 25.99 %. The most critical failure type has been found to be abrasive wear which is 0.1 mm in depth along 100 mm length for 8×19 Warrington rope with independent wire rope core where lifting capacity reduced by 7.93 %.